Solid-state JEOL 300 MHz NMR spectrometer with broadband MAS probe

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Solid-state JEOL 300 MHz NMR spectrometer with broadband MAS probe

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Documents and Tutorials


JEOL manuals

  •  General principles are described in the Liquids Manual
  • Specific operations involved in the solid-state are covered in the Solids Manual. However, to be able to use this manual you must first go through the Liquids Manual
  • Description of the JEOL sample tube (rotor) is given in the Sample Tube Manual

Solid-state NMR Reading

  • The tutorial Solid-state NMR tutorial by Michael Frey of JEOL concisely touches on all necessary step and considerations of the solid-state NMR.
  • Good books that we strongly recommend to have in the lab:

    • Solid-State NMR: Basic Principles and Practice by David C. Apperley, Robin K. Harris, Paul Hodgkinson  (any edition is good)
    • Introduction to Solid-State NMR Spectroscopy by Melinda J. Duer (any edition is good)

Notre Dame Tutorials


Step-by-Step Protocol

  1. Load the sample tube and pack the sample on the benchtop spinner
  2. Acquire NMR data