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Variable-temperature NMR operation

 


 

 

Contents

 

General Training for Bruker 400 MHz (Stepan) and 500 MHz (McCourtney) NMR spectrometers


 

 

 

 

 

 

 

 

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General Training for Bruker 400 MHz (Stepan) and 500 MHz (McCourtney) NMR spectrometers

 

Mandatory training sequence (prerequisite to all specific setup guides)

Software Control

 

 

 

Back to General Training for Bruker 400 and 500

 


   Critical Warnings and Precautions

This is the first mandatory part for VT training for all NMR users at Notre Dame.

https://youtu.be/pZ_FaQw1fBM

 

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  Handling of a Ceramic Spinner

This tutorial is a mandatory part for VT training for all NMR users at Notre Dame.

https://youtu.be/x-xSGb7L398

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  Shim Gas - turning on and off

This tutorial is a mandatory part for VT training for all NMR users at Notre Dame

https://youtu.be/-obFZrys994

 

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  Design and Use of a Liquid Nitrogen Chiller

This video describes design and use of the liquid N2 chiller

https://youtu.be/s9FoIvHPNRY

 

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    Introduction to Variable Temperature Operation

This tutorial is a mandatory part for VT training for all NMR users at Notre Dame.

https://youtu.be/wyJ7Kdb_R1Q

 

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   High Temperature Operation on Stepan 400 and McCourtney 500

Prerequisites:

 

Print this checklist (same for 400 and 500 MHz) and bring with you to NMR room: High-temperature checklist

 

 

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   Moderate Low Temperature Operation on Stepan 400

This tutorial covers VT operation on Stepan 400 equipped with manual BCU-1 cooling unit

 

Prerequisites:

 

 

https://youtu.be/g5A3cFSSi5s

 

 

Print this checklist and bring with you to NMR room: Moderate low temperature checklist

 

 

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   Moderate Low Temperature Operation on McCourtney 500

Prerequisites:

This topic does not have a dedicated video tutorial. Please, watch: Moderate Low Temperature Operation on Stepan 400

and print this checklist to bring with you to NMR room: Moderate Low Temperature 500 checklist

 

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   Ultra-low temperature operation on Stepan 400

This is a tutorial for ultra-low temperature training on Bruker 400 MHz instrument in Stepah

Prerequisites:

 

 

 

Part 1

https://youtu.be/iw7gB1TZCAI

 

 

Part 2

https://youtu.be/0e0S0XHO-Vc

 

Print this checklist and bring with you to NMR room: Ultra-low temperature checklist

 

 

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   Using EDTE to control temperature

This is a tutorial covering control  of the variable temperature operation through Topspin EDTE utility.

Prerequisites:

 

 

 

https://youtu.be/HD5XbFgTWvk

 

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