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Temperature calibrations:
Stepan 400, probe ID 0557 repaired in 2024

Below you will find overview graphs as well as graphs zoomed into specific regions. Please, use zoomed graphs for more accurate calibrations. 

These calibrations were obtained by EK in February of 2024 for after the probe 0557 was returned from repair by Bruker. The original data are from EK442.Stepan_400.Temp_Calibration.0557_after_repair/.

 

Stepan 400/0557: Overview

Black points: calibration data
Red line: reference 1:1 line to guide an eye

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Stepan 400/0557: High-temperature branch

 

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Stepan 400/0557: High-temperature no-trust region

Do NOT set:  VTU = 330.0 to 331.0 corresponding to a "dead region"  of inaccessible T (real) = 333.0 K to 338.2 K

 

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Stepan 400/0557: Moderate region (including no-trust regions and zoomed center)

Black points: calibration data
Red line: reference 1:1 line to guide an eye

 

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Stepan 400/0557:  low-temperature no-trust region

Do NOT set VTU between 278.0 to 279.0: corresponding to a "dead region"  of inaccessible T (real) = 273.5 K to 276.7K

Black points: calibration data
Red line: reference 1:1 line to guide an eye

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Stepan 400/0557: Low-temperature branch and extrapolation graph

Black points: calibration data
Red line: reference 1:1 line to guide an eye

Full data range graph

NOTE: the lowest point of the range is temperature when methanol standard freezes in the probe and can no longer be detected.

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Extrapolation to the ultra-low region

Linear extrapolation to the probe lower limit (-150C)

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